Развитие метода кинетической радиофлуорометрии для исследований ион-радикалов и их реакций в облученных неполярных растворах
Диссертация
О предмете диссертации. Известно, что одной из форм отклика органического раствора на облучение является задержанная флуоресценция раствора. Энергия ионизирующей частицы частично трансформируется в энергию кулоновского взаимодействия противоположно заряженных ионов и, затем, в энергию электронного возбуждения продуктов их рекомбинации. Очевидно, что кинетика индуцированного радиацией… Читать ещё >
Содержание
- 1. Обзор литературы
- 1. 1. Общие представления о развитии исследований радиофлуоресценции и радиационно-инициированных процессов
- 1. 2. Сверхвозбужденные состояния молекул
- 1. 3. Формирование трека ионизирующей частицы. Термализация избыточных электронов
- 1. 4. Структура трека ионизирующей частицы
- 1. 5. Избыточный электрон в алкановых растворах
- 1. 6. Исследования катион-радикалов алканов
- 1. 6. 1. Катион-радикалы алканов в низкотемпературных матрицах
- 1. 6. 2. Катион-радикалы алканов в растворах
- 1. 7. Органические ион-радикалы в растворах
- 1. 8. Диффузионное движение молекулярных частиц в растворах
- 1. 9. Сведения о теории активированных процессов
- 1. 10. Кинетика диффузионно-контролируемых процессов
- 1. 11. Экспериментальные методы исследования первичных носителей заряда в облученных алканах
- 1. 11. 1. Метод импульсного радиолиза с оптической регистрацией промежуточных частиц
- 1. 11. 2. Измерение наведенной проводимости
- 1. 11. 3. Измерение кинетики радиофлуоресценции облученных растворов
- 2. 1. Метод времяразрешенного электрического эффекта (ВЭЭ)
- 2. 2. Метод «дорекомбинациониого» тушения
- 2. 3. Метод времяразрешенного магнитного «эффекта «(ВМЭ) Т. Г... .77тгТ?>?
- 2. 4. Описание экспериментальной установки
- 3. 1. Подход и алгоритм
- 3. 2. Проявление многочастичных эффектов
- 4. 1. Моделирование кинетики рекомбинации избыточных электронов
- 4. 2. Исследование реакции захвата избыточных электронов в к-додекане
- 4. 3. Исследование обратимого присоединения электронов к молекулам с применением метода ВЭЭ
- 5. 1. Регистрация и изучение КР алканов в растворах
- 5. 1. 1. Эксперимент
- 5. 1. 2. Катион-радикалы нормальных алканов
- 5. 1. 3. Катион-радикалы разветвленных алканов
- 5. 2. Реакции переноса электрона с участием
- 5. 2. 1. Перенос электрона от молекул аминов
- 5. 2. 2. Исследование переноса электрона с применением метода ВМЭ
- 5. 2. 3. Вырожденный электронный обмен
- 5. 2. 4. Реакции переноса протона
- 5. 2. 5. Парамагнитная релаксация КР циклоалканов
- 6. 1. Исследование вторичных анион-радикалов
- 6. 2. Катион-радикалы вторичных соединений
- 6. 2. 1. Катион-радикалы элементоорганических алифатических соединений
- 6. 2. 2. Наблюдение мономолекулярного распада вторичных ион-радикалов
- 6. 3. Диффузия органических ион-радикалов в алкановых растворах
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