Строение и транспортные свойства SrFe1-xMxO3-z (M=Mo, W) перовскитов
Диссертация
Возможность стабилизации кубической фазы феррита методом парциального замещения железа на Ti, Ga, Al, Sc и влияние допирования^ на транспортные характеристики изучались в ряде работ. Как правило, наилучшие транспортные характеристики вдопированных производных достигаются при минимальных концентрациях замещающего ' катиона, обеспечивающих стабилизацию кубической фазы. Можноожидать, что при… Читать ещё >
Содержание
- ВВЕДЕНИЕ.4'
- Глава 1. Литературный обзор
- 1. 1. Структура перовскитоподобных оксидов!
- 1. 2. Структура феррита стронция
- 1. 3. Электрохимическое окисление феррита стронция при комнатной температуре
- 1. 4. Микроструктура нестехиометрических и замещенных перовскитов
- 1. 5. Кислородный транспорт в нестехиометрических перовскитах
- 1. 5. 1. Теория окисления Вагнера. Диффузионный режим
- 1. 5. 2. Модель Эрлиха: Кинетическийрежим *
- 1. 5. 3. Характеристическая толщина мембраны
- 1. 5. 4. Кислородная проницаемость SriyAyFeixBxQ3. z (A=La, .Ca- B=Ti, Al- Co) перовскитов
- 2. 1. Методььсинтеза-нестехиометрических перовскитов SrFe^M'xO^z
- 2. 2. Определение содержания кислорода в образцах SrFeixMx03. z (М=Мо, W)
- 2. 3. Определение содержания молибдена и вольфрама в образцах.60 j
- 2. 4. Рентгеновский анализ*.6Г
- 2. 4. 1. Исследование микроструктуры и размеров кристаллитов по интегральной* ширине дифракционных линий
- 2. 4. 2. Высокотемпературные дифракционные исследования
- 2. 5. Термогравиметрический анализ
- 2. 6. Хронопотенциометрические исследования
- 2. 7. Мессбауэровская спектроскопия
- 2. 8. Сканирующая электронная микроскопия и электронная микроскопия высокого разрешения
- 2. 9. Высокотемпературные исследования кислородной проницаемости
- 4. 1. Структурные исследования SrFeixMox03. z на воздухе
- 4. 2. Высокотемпературные исследования SrFeixMox03. z в вакууме
- 4. 3. Термомеханические свойства SrFe^JMOxOa.z перовскитов
- 4. 4. Иселедования термической стабильности SrFeixMx03z (М=Мо, W- 0<х<0.5) перовскитов
- 5. 1. Хронопотенциометрические исследования SrFe[xMx03z (М=Мо, W) перовскитов
- 5. 2. Ионная и электронная проводимость феррита стронция, допированного молибденом и вольфрамом
- 5. 3. Кислородная проницаемость керамических мембран на основе нестехиомет-рических перовскитов состава SrFeixMx03z (М=Мо, W- 0<х<0.1)
- 5. 4. Каталитическая активность SrFei. xMx03.z (М=Мо, W- 0<х<0.1) в реакциях окисления метана
- 5. 5. Характеризация поверхностей мембран
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