Жидкофазный синтез ацетато-, оксалато-и гидроксотитанилов некоторых nS2 металлов, физико-химические характеристики их термических превращений и электрореологические свойства
Титанаты бария, стронция и кальция представляют собой перспективный класс материалов с сегнетои параэлектрическими свойствами, нашедших широкое применение в качестве активных элементов пьезоэлектрических преобразователей, оптических модуляторов, сегнетоэлектрических запоминающих устройств, конденсаторов с высокой диэлектрической постоянной, СВЧ-устройств, фотокатализаторов. Миниатюризация изделий… Читать ещё >
Содержание
- 1. ЛИТЕРАТУРНЫЙ ОБЗОР
- 1. 1. Структура титанатов
- Структурно-фазовые переходы в сегнетоэлектриках на примере титаната бария
- 1. 3. Диэлектрическая проницаемость
- 1. 4. Размерный эффект в сегнетоэлектриках
- 1. 5. Методы синтеза наноразмерных материалов
- 1. 5. 1. Твердофазный метод синтеза
- 1. 5. 2. Метод пиролиза
- 1. 5. 3. Механохимический метод синтеза ^ ^ Жидкофазные методы синтеза сегнетоэлектрических ^ материалов
- 1. 5. 5. Метод (Печини) полимерного прекурсора
- 1. 5. 6. Гидротермальный метод
- 1. 5. 7. Оксалатный метод
- 1. 5. 8. Золь-гель метод
- 1. 5. 9. Низкотемпературный синтез
- 1. 5. 10. Электрохимический метод
- 1. 6. Умные материалы
- 1. 7. Электрореологические жидкости
- Неорганические наполнители электрорсологических жидкостей
- I. у 2 Органические наполнители электрореологических 45 жидкостей у 2 Гибридные наполнители электрореологических 47 материалов
- 1. 7. 4. Поверхностно-активные вещества
- I. у 5 Мезопористые наполнители электрореологических 49 жидкостей
- 1. 8. Механизмы электрореологического эффекта
- 1. 8. 1. Механизм поляризации
- 1. 8. 2. Механизм Максвелла-Вагнера
- 1. 8. 3. Модель водных мостов
- 1. 8. 4. Механизм проводимости
- 1. 9. Реологические аспекты электрореологического эффекта
- 1. 8. Механизмы электрореологического эффекта
- Обоснование выбора сегнетоэлектрических материалов в
- 1. 10. качестве дисперсной фазы электрореологически активных 57 жидкостей
- 2. ЭКСПЕРИМЕНТАЛЬНАЯ ЧАСТ
- 2. 1. Показатели качества используемых веществ и реагентов
- Методы синтеза наноразмерных материалов
- 2. 2. ацетатотитанилов бария, стронция, кальция и смешанные 61 формы, оксалатотитанил бария, гидроксотитанила бария
- 2. 2. 1. Синтез порошка ВаТЮ (СН3СОО)
- 2. 2. 2. Синтез порошка ВаТЮ (С204)
- 2. 2. ацетатотитанилов бария, стронция, кальция и смешанные 61 формы, оксалатотитанил бария, гидроксотитанила бария
- 2. 2. 4. Синтез ацетатотитанила бария-стронция и бария-кальция
- 2. 2. 5. Синтез ацетатотитанила стронция
- 2. 2. 6. Синтез ацетатотитанила кальция
- 2. 3. Описание методов исследования физико-химических свойств материалов
- 2. 3. 1. Просвечивающая электронная микроскопия
- 2. 3. 2. Атомно-силовая микроскопия
- 2. 3. 3. Инфракрасная спектроскопия
- 2. 3. 4. Рентгепофазовый анализ
- 2. 3. 5. Термический анализ
- 2. 3. 6. Дифференциальная сканирующая калориметрия
- 2. 3. 7. Низкотемпературная адсорбция/десорбция азота
- 2. 3. 8. Диэлектрические измерения
- 2. 3. 9. Электрореологические измерения
3 ^ з Физико-химические характеристики синтезированного gQ порошка ВаТіОз в щелочной среде Физико-химические характеристики синтезированного 3.1.4. золь-гель методом ацетатотитанила бария-стронция и бария-кальция
Физико-химические характеристики синтезированного ^ золь-гель методом ацетатотитанила стронция и кальция 3 2 Анализ диэлектрических характеристик и исследование | эффективности применения полученных материалов в качестве наполнителем электрореологических жидкостей 30% суспензий полученных материалов в силиконовом масле ПМС
2 2 і Электрореологические и диэлектрические характеристики ^ ^ суспензий с дисперсной фазой ВаТіО (СН3СОО)
3 2 2 Электрореологические и диэлектрические характеристики | ^ суспензий с дисперсной фазой ВаТЮ (С204)2 Электрореологические и диэлектрические характеристики суспензий с дисперсной фазой порошка ВаТіОз в 11 щелочной среде
Электрореологические и диэлектрические характеристики 3.2.4. суспензий с дисперсной фазой ацетатотитанила бария- ' ^ ^ стронция и бария-кальция
Электрорсологические и диэлектрические характеристики т о с і ОД суспензий с дисперсной фазой ацетатотитанила стронция и кальция
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