Высокоупорядоченные двумерные ансамбли наночастиц металлов: управление структурой и плазмонно-резонансные свойства
Диссертация
Проблема конструирования высокоупорядоченных двумерных ансамблей наночастиц (НЧ) металлов (в первую очередь, — благородных) приобрела особую значимость к концу 90-тых годов. Именно в это время стало очевидным, что такие ансамбли могут быть использованы в качестве рабочих элементов как хемои биосенсоров, так и ряда устройств нанооптики и нанофо-тоники, функционирующих на эффекте локализованного… Читать ещё >
Содержание
- Список сокращений
- Глава 1. Обзор литературы
- 1. 1. Введение
- 1. 2. Методы формирования двумерных упорядоченных ансамблей 8 НЧ
- 1. 3. Формирование высокоупорядоченных ансамблей наночастиц 12 металлов с использованием мицелл дифильных диблоксополиме
- 1. 3. 1. Мицеллярные растворы и пленки диблоксополимеров
- 1. 3. 2. Формирование упорядоченных ансамблей НЧ на твердых 15 подложках
- 1. 4. Зависимость ЛППР от геометрии ансамблей НЧ
- 1. 5. Практические применения двумерных упорядоченных 22 ансамблей НЧ металлов
- Глава 2. Методическая часть
- 2. 1. Реактивы и материалы
- 2. 2. Конструирование упорядоченных планарных ансамблей нано- 25 частиц
- 2. 3. Методы исследования
- Глава 3. Результаты и их обсуждение
- 3. 1. Исследование поведения диблоксополимеров в растворе
- 3. 2. Мицеллярные пленки
- 3. 2. 1. Влияние введение прекурсора металла в растворы ДБС на 37 структуру их мицеллярных пленок
- 3. 2. 2. Методы управления характеристическими размерами моно- 44 мицеллярных пленок ДБС
- 3. 3. Формирование ансамбля наночастиц металла
- 3. 3. 1. Восстановление прекурсора металла и удаление полимера. 50 Анализ химического состояния поверхности образцов
- 3. 3. 2. Химические способы восстановления прекурсора в мицеллах 57 ДБ С
- 3. 3. 3. Методы управления плотностью упаковки и размером НЧ в 61 их двумерном ансамбле
- 3. 4. Доращивание (укрупнение) НЧ в их двумерном ансамбле
- 3. 4. 1. Одностадийный метод доращивания
- 3. 4. 2. Интервальный метод доращивания
- 3. 4. 3. Влияние размера НЧ 20-упорядоченного ансамбля на его 75 плазмонно-резонансные свойства
- 3. 4. 4. Формирование серебряной оболочки на НЧ золота
- 3. 5. Конструирование ансамбля НЧ на поверхности полимер- 84 ных подложек
- 3. 5. 1. Зависимость геометрии ансамбля от характера и степени де- 85 формации подложки
- 3. 5. 2. Зависимость положения ЛППР от расстояния между НЧ
- 3. 5. 3. Конструирование двумерных композитов «полимер-металл»
- 3. 6. Золь-гель синтез ансамблей НЧ кремнезема с использова- 101 нием мицелл ДБС
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